Evaluation of Mechanical and Microstructural Properties of Mortar Reinforced with Carbon Nanotubes at Elevated Temperatures
Abstract
An experimental study was performed to analyze the effect of multi-walled carbon nanotubes (MWCNT’s) on preheated and post heated mechanical properties of cement mortar. Cement was replaced with 0.125%, 0.25%, 0.375%, and 0.5% MWCNT’s and mortar cubes were then subjected to 25oC, 400oC, and 800oC after 90 days of curing to determine the residual compressive strength. Microstructural analysis was performed on pre-heated and post-heated samples to identify changes in hydration products and decomposition phases by using scanning electron microscopy (SEM). Mortar samples heated at 400oC showed slight changes in microstructure but became more evident at 800oC. Tests performed on pre-heated samples show that the addition of 0.125% in cement as an optimum dosage can increase mortar strength up to 53.4% due to the bridging effect of CNT’s which improve load distribution, however higher dosages of CNT’s lead to a decrease in strength as compared to optimum mix. It has been determined that higher dosages of CNT’s (0.375% and 0.5%) enhanced relative compressive strength of mortar up to 26.3% and 66.9% respectively at 400oC. Similarly, the addition of 0.375% and 0.5% CNT’s improved residual compressive strength by 23.64% and 61.4% respectively at 800oC due to reduction in the size of cracks and formation of compact and stable microstructure as observed from SEM images. Besides, an increase in the dosage of CNT’s provide sufficient resistance against spalling and reduction in mass of mortar at elevated temperatures.
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